A strategy for the protection and deprotection of sensitive secondary amines is based on this principle.
12.
This prevented loss of ee before deprotection with tetra-n-butylammonium fluoride ( TBAF ).
13.
The main complications are to perform the deprotection step without racemization and to form a pure salt.
14.
The general principle of SPPS is one of repeated cycles of deprotection-wash-coupling-wash.
15.
The TES group is later removed in the concluding silyl deprotection step that gives the final Taxol compound.
16.
Boc SPPS uses special equipment to handle the final cleavage and deprotection step, which requires anhydrous hydrogen fluoride.
17.
The deprotection step can lead to four distinct chemical functionalities, two of which are promising for increasing conductivity.
18.
Provided the monosaccharide amino acid building block is stable to peptide coupling conditions, amine deprotection conditions and resin cleavage.
19.
Their removal merely consists of increasing temperature, which leads to deprotection of the protected sensitive part of a molecule.
20.
It was first prepared by the reaction of chlorodiphenylphosphine with the Grignard reagent derived from the protected bromobenzaldehyde followed by deprotection.
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