A breakthrough in SAXS and SANS experiments came in the 1970s, thanks to the availability of synchrotron radiation and neutron sources, the latter paving the way for contrast variation by solvent exchange of H 2 O for D 2 O and specific deuteration methods.
12.
They replicated the earlier results of Vosshall and Keller showing that humans cannot reliably distinguish between acetophenone and its deuterated counterpart, with 8 hydrogens, and showed that humans only begin to detect the isotope odor of the musks beginning at 14 deuteriums, or 50 % deuteration.
13.
Characterization of peptide B1 as full CROP domain of TcdB by HDX-MS reveal that fragment corresponding to residues 1902-1914, 2021-2025, 2033-2038 and 2091-2096 appear to have a strong interaction with bezlotoxumab, as denoted by the minimal levels of deuteration.
14.
It is also home to the National Deuteration Facility, which runs a user service providing both bio-synthesis and bottom-up organic synthesis of molecules for use in neutron scattering, triple-labelled NMR, and other studies, and operates two small-angle X-ray scattering instruments and an X-ray reflectometer.
15.
It should be noted, however, that deuteration changes the heats of adsorption and the boiling and freezing points of molecules ( boiling points : 100.0 �C for H 2 O vs . 101.42 �C for D 2 O; melting points : 0.0 �C for H 2 O, 3.82 �C for D 2 O ), p " K " a ( i . e ., dissociation constant : 9.71?0 " 15 for H 2 O vs . 1.95?0 " 15 for D 2 O, cf.
16.
It should be noted, however, that deuteration changes the heats of adsorption and the boiling and freezing points of molecules ( boiling points : 100.0 �C for H 2 O vs . 101.42 �C for D 2 O; melting points : 0.0 �C for H 2 O, 3.82 �C for D 2 O ), pKa ( i . e ., dissociation constant : 9.71x10 " 15 for H 2 O vs . 1.95x10 " 15 for D 2 O, cf . heavy water ) and the strength of hydrogen bonding.
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