Proof-of-concept work has been done with microfluidics, in which continuous point-of-use synthesis from N-methyl-N-nitrosourea and 0.93M potassium hydroxide in water was followed by point-of-use conversion with benzoic acid, resulting in a 65 % yield of the methyl benzoate ester within seconds at temperatures ranging from 0-50 C . The yield was better than under capillary conditions; the microfluidics were credited with " suppression of hot spots, low holdup, isothermal conditions, and intensive mixing ."
12.
Secondly, I notice there isn't a lot in this workup that separates methyl benzoate and bromobenzene from the product . . . is it reasonable that they all get consumed to near completion ( I had an MP depression of about 5 C ); their BPs are really high but the product is a solid; maybe bromobenzene and methyl benzoate form an azeotrope that can be evaporated easily . . . ? ( But on a totally different scale than evaporating ether . ) Would acid-catalysed hydrolysis of the starting reagent into methanol and benzoic acid help significantly ? talk ) 04 : 22, 20 October 2009 ( UTC)
13.
Secondly, I notice there isn't a lot in this workup that separates methyl benzoate and bromobenzene from the product . . . is it reasonable that they all get consumed to near completion ( I had an MP depression of about 5 C ); their BPs are really high but the product is a solid; maybe bromobenzene and methyl benzoate form an azeotrope that can be evaporated easily . . . ? ( But on a totally different scale than evaporating ether . ) Would acid-catalysed hydrolysis of the starting reagent into methanol and benzoic acid help significantly ? talk ) 04 : 22, 20 October 2009 ( UTC)
How to say methyl benzoate in Hindi and what is the meaning of methyl benzoate in Hindi? methyl benzoate Hindi meaning, translation, pronunciation, synonyms and example sentences are provided by Hindlish.com.
