After enough titrant has been added to react completely with the analyte, the excess titrant may itself be reduced at the working electrode.
22.
After enough titrant has been added to react completely with the analyte, the excess titrant may itself be reduced at the working electrode.
23.
Successful applications for thermometric titrations are generally where titrant-titrand reaction kinetics are fast, and chemical equilibria are stoichiometric or nearly so.
24.
The chief advantage over other types of titration is the selectivity offered by the electrode potential, as well as by the choice of titrant.
25.
Measured volumes of titrant are added, with thorough ( magnetic ) stirring, and the corresponding values of emf ( electromotive force ) or pH recorded.
26.
Under these conditions, for a constant rate of titrant addition the temperature increase is constant and the curve is essentially linear until the endpoint is approached.
27.
After the equivalence point "', the solution will contain two bases : the conjugate base of the acid and the strong base of the titrant.
28.
I use the volume of titrant NaOH added, rather than the pH value, to calculate the concentration of unknown NaOH . Here's method one.
29.
Where reaction kinetics are slow, and direct titrations between titrant and titrand are not possible, indirect or back-titrations often can be devised to solve the problem.
30.
The titration shown here with an acidic titrant, such as HCl, is the reverse of the original picture in titration, in which apparently a basic titrant is used with phenolphthalein.
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